反応 #2320084

ord-f2ad587226ea410b8bc263f65cc14c20

反応方程式

N#Cc1cc(N2CCNCC2)ccc1F
2-fluoro-5-piperazin-1-yl-benzo-nitrile
CCCI
1-iodopropane
CCCN1CCN(c2ccc(F)c(C#N)c2)CC1
2-Fluoro-5-(4-propyl-piperazin-1-yl)-benzonitrile

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他the title compound was recovered by the procedure

実験手順

Beginning with 2-fluoro-5-piperazin-1-yl-benzo-nitrile and 1-iodopropane, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 247 (M+, 25), 218 (bp), 175 (28), 147 (33), 70 (65).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: USRE041315E1uspto-grants-2010_05