反応 #2320080

ord-3fee12487f424da98d34f9e6c26fe511

反応方程式

FC(F)(F)c1cc(C2CCNCC2)ccc1Cl
4-(4-Chloro-3-trifluoromethyl-phenyl)-piperidine
CCCCBr
1-butylbromide
CCCCN1CCC(c2ccc(Cl)c(C(F)(F)F)c2)CC1
4-(4-Chloro-3-trifluoromethyl-phenyl)-1-butyl-piperidine

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他the title compound was recovered by the procedure

実験手順

Beginning with 4-(4-Chloro-3-trifluoromethyl-phenyl)-piperidine and 1-butylbromide, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 319 (M+, 6), 278 (31), 277 (19), 276 (bp), 70 (30).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: USRE041315E1uspto-grants-2010_05