反応 #2314285

反応方程式

water

boron tribromide

anisole

2-(4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)ethyl-4-methoxybenzene

→

4-[2-(4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)ethyl]phenol

溶媒

dichloromethane

反応条件

後処理

1. 1
   抽出The reaction mixture is extracted with dichloromethane
2. 2
   乾燥dried over magnesium sulfate
3. 3
   濃縮The solution is concentrated in vacuo
4. 4
   その他The product is recrystallized from hexane

実験手順

To a solution of anisole 2F (R=4-Methyl-3-pentenyl) (6 g) in dichloromethane (100 mL) and cooled in an ice bath is added a 1M solution of boron tribromide (3.4 mL). The solution is stirred for one hour, then poured into water. The reaction mixture is extracted with dichloromethane and dried over magnesium sulfate. The solution is concentrated in vacuo. The product is recrystallized from hexane.

出典