反応 #2314282

反応方程式

acid 2B

(4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)acetic acid

oxalyl chloride

→

(4-(4-Methyl-3-pentenyl)-3-cyclohexenyl)acetyl chloride

反応条件

後処理

1. 1
   workup.ADDITIONTo a 100 mL flask containing a stirbar
2. 2
   その他Residual oxalyl chloride is removed in vacuo

実験手順

To a 100 mL flask containing a stirbar is added the acid 2B (R=4-Methyl-3-pentenyl) (10 g) and oxalyl chloride (8.3 mL). The reaction is stirred under a nitrogen atmosphere for one hour after gas evolution ceases. Residual oxalyl chloride is removed in vacuo.

出典