反応 #2314274

反応方程式

N-dimethylsulfamoylimidazole

t-BuLi

zinc chloride

→

N-dimethylsulfamoyl-imidaz-2-yl zinc chloride

溶媒

THF

反応条件

実験手順

N-dimethylsulfamoyl-imidaz-2-yl zinc chloride was prepared in situ by lithiation of N-dimethylsulfamoylimidazole (0.97 g, 5.5 mmol) in THF (20 mL) with t-BuLi ( 1.7M, 6.7 mL), followed by quenching with zinc chloride (1.87 g, 13.75 mmol).

出典