反応 #2313821

ord-fe283c62451a4af996aa22700980c600

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The precipitated while solid
  2. 2
    洗浄was washed with ether
  3. 3
    その他dried

実験手順

34.13 g (0.1 mol) of N-benzylpyridinium tosylate obtained in Example 1 was dissolved in 100 of water, and was added to 25.88 g (0.1 mol) of sodium hexafluoroantimonate. The precipitated while solid was washed with ether and dried to give the titled compound. Yield: 72%.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05349067uspto-grants-1994_09