反応 #2307979
ord-783ff6d15d5d4dcd91d81b830e764a32
反応方程式
triethylene glycol
compound 31
20-methoxy-1-(methylsulfonyl)oxy-3,6,9,12,15,18-hexaoxaeicosane
methanol
→
compound 32
Decaethylene glycol monomethyl ether
反応物
試薬
なし
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Monodispersed compound 32 was prepared from compound 31 and monodispersed triethylene glycol using the procedure described above in Example 17. Oil; Rf 0.41 (methanol: chloroform=6:10); MS m/z calc'd for C21H44O11 472.29 (M++1), found 472.29.