反応 #2281

反応方程式

p-chlorobenzoic hydrazide

chloroacetyl chloride

→

N'-chloroacetyl-4-chlorobenzoic hydrazide

溶媒

dioxane

反応条件

後処理

1. 1
   温度The resulting mixture was refluxed for three hours
2. 2
   ろ過filtered
3. 3
   洗浄The resulting solid was washed with ethyl ether
4. 4
   その他dried

実験手順

To a solution of p-chlorobenzoic hydrazide (11.2 g) in dioxane (100 ml) was added chloroacetyl chloride (6 ml). The resulting mixture was refluxed for three hours, cooled to room temperature and filtered. The resulting solid was washed with ethyl ether and dried to yield N'-chloroacetyl-4-chlorobenzoic hydrazide as white solid.

出典