反応 #2267072

反応方程式

compound 10

4-Methoxy-3-nitrophenylacetone

→

desired product 11

収率 94.0%

3-Amino-4-methoxyphenylacetone

収率 94.0%

溶媒

ethanol

反応条件

後処理

1. 1
   ろ過Filtration of the catalyst and evaporation of solvent

実験手順

The mixture of compound 10 (3.0 g, 14.3 mmol) and 10% palladium on carbon (1.6 g) in ethanol (230 ml) was stirred under hydrogen for 3 hours. Filtration of the catalyst and evaporation of solvent gave desired product 11 (2.41 g, 94%).

出典