反応 #2267059

反応方程式

tetramethylammonium hydroxide

pentafluorobenzenesulfonyl chloride

→

tetramethylammonium pentafluorobenzenesulfonate

溶媒

methanol

反応条件

後処理

1. 1
   workup.ADDITIONwas slowly added

実験手順

In 100 ml of methanol was dissolved 25 g of pentafluorobenzenesulfonyl chloride under cooling with ice, and 100 g of an aqueous solution of 25% tetramethylammonium hydroxide was slowly added thereto. The mixture was stirred for 3 hours at room temperature to obtain a solution of tetramethylammonium pentafluorobenzenesulfonate. The solution was used for salt-exchange with a sulfonium salt or an iodonium salt.

出典