反応 #2205694

ord-9f48bc15626348a09cde45fba99d0310

反応方程式

COc1cc2c(cc1OC)CCN=C2
6,7-dimethoxy-3,4-dihydro-isoquinoline
Cc1ccc(CCl)cc1
4-methylbenzyl chloride
→
COc1cc2c(cc1OC)CC[N+](Cc1ccc(C)cc1)=C2.[Cl-]
title compound
COc1cc2c(cc1OC)CC[N+](Cc1ccc(C)cc1)=C2.[Cl-]
2-(4-Methylbenzyl)-6,7-dimethoxy-3,4-dihydroisoquinolinium chloride

反応物

COc1cc2c(cc1OC)CCN=C2
6,7-dimethoxy-3,4-dihydro-isoquinoline
Cc1ccc(CCl)cc1
4-methylbenzyl chloride

試薬

なし

溶媒

ClCCCl
ethylene chloride

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The title compound is prepared analogously to Example A from 6,7-dimethoxy-3,4-dihydro-isoquinoline and 4-methylbenzyl chloride in ethylene chloride. Melting point: 181°-183° C. (Decomp.)

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04678792uspto-grants-1987_07