反応 #2200579

反応方程式

ethyl 4-chloro-3-hydroxybutyrate

DMCS

→

Ethyl 4-Chloroacetoacetate

反応条件

後処理

1. 1
   その他was carried out at 150° C

実験手順

The quantitation of ethyl 4-chloro-3-hydroxybutyrate was carried out by gas chromatography. Thus, using a glass column (ID 3 mm×1 m) packed with PEG-20M Chromosorb WAW DMCS 10%, 80/100 mesh (product of GL Sciences Inc.), chromatography was carried out at 150° C. The detection was made by FID.

出典