反応 #2195502

反応方程式

product

9-Benzyl-7,7,11,11-tetrafluoro-1,5-dithia-9-azaspiro[5.5]undecane

→

title compound

1-Benzyl-3,3,5,5-tetrafluoropiperidine

反応条件

後処理

1. 1
   その他purify by silica gel chromatography

実験手順

React 4.0 mmol of the product of Example 29 with Raney nickel according to the general procedure set forth in Example 23 and purify by silica gel chromatography using methylene chloride/methanol/saturated NH4OH as eluant to yield the title compound.

出典