反応 #219271

反応方程式

1-dodecene

formic acid

H2O2

→

1,2-Dodecanediol

溶媒

ethanol

反応条件

後処理

1. 1
   その他the main fraction obtained after the workup
2. 2
   workup.DISTILLATIONby distillation

実験手順

336 g (2.00 mol) of 1-dodecene were reacted with 236 g of formic acid and 185 g of a 50% strength aqueous H2O2 solution in accordance with Example 4. 412 g of ethanol were employed for the Marlon AS3 acid-catalyzed transesterification, and the main fraction obtained after the workup by distillation was 99.5% pure, virtually odorless 1,2-dodecanediol.

出典