反応 #2186215

反応方程式

thioanisole

dimethyl sulfate

water

→

Dimethylphenylsulfonium Hydrogen Sulfate

溶媒

diethyl ether

反応条件

後処理

1. 1
   その他separated into two layers

実験手順

6.2 g (0.05 mole) of thioanisole and 6.9 g (0.055 mole) of dimethyl sulfate were stirred for 12 hours at room temperature. 100 g of water and 50 ml of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, dimethylphenylsulfonium hydrogen sulfate.

出典