反応 #2186212

ord-c4adb02f875649e5b49181e1d4a3888a

反応方程式

Cc1ccc(S(=O)c2ccc(C)cc2)cc1
bis(4-methylphenyl) sulfoxide
Cc1ccc(Cl)cc1
4-chlorotoluene
Cc1ccc([S+](c2ccc(C)cc2)c2ccc(C)cc2)cc1.[Cl-]
tris(4-methylphenyl)sulfonium Chloride

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The target compound was obtained
  2. 2
    その他the procedure of Synthesis Example 1 aside
  3. 3
    その他in Synthesis Example 1
  4. 4
    抽出for extraction

実験手順

The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-methylphenyl) sulfoxide instead of the diphenyl sulfoxide and 4-chlorotoluene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07569326B2uspto-grants-2009_08