反応 #218285

反応方程式

intermediate 1.10

10H-phenothiazine-2-carboxylic acid

1-(5-acetyl-10,11-dihydro-5H-dibenzo[b,f]azepin-3-yl)ethanone

→

5-acetyl-10,11-dihydro-5H-dibenzo[b,f]azepine-3-carboxylic acid

収率 62.0%

反応条件

後処理

1. 1
   その他A pale yellow solid is obtained with a yield of 62%

実験手順

The experimental protocol used is the same as that described for the synthesis of intermediate 1.10, using 1-(5-acetyl-10,11-dihydro-5H-dibenzo[b,f]azepin-3-yl)ethanone (J. Chem. Soc. 1973, 859-863) as starting product. A pale yellow solid is obtained with a yield of 62%. Melting point: 189-189.5° C.

出典