反応 #2161235

反応方程式

phenacyl bromide

tetrahydrothiophene

water

diethyl ether

→

Phenacyltetrahydrothiophenium Bromide

溶媒

nitromethane

反応条件

後処理

1. 1
   その他separated into two layers

実験手順

88.2 g (0.44 mole) of phenacyl bromide and 39.1 g (0.44 mole) of tetrahydrothiophene were dissolved in 220 g of nitromethane, which was stirred for 4 hours at room temperature. 800 g of water and 400 g of diethyl ether were added to the reaction solution whereupon the mixture separated into two layers. The aqueous layer was taken out, which was an aqueous solution of the target compound, phenacyltetrahydrothiophenium bromide.

出典