反応 #2161233

ord-c2309b402e6a48dd9264b46b3541b9e5

溶媒

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他The target compound was obtained
  2. 2
    その他the procedure of Synthesis Example 1 aside
  3. 3
    その他in Synthesis Example 1
  4. 4
    抽出for extraction

実験手順

The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-methylphenyl)sulfoxide instead of the diphenyl sulfoxide and 4-chlorotoluene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07919226B2uspto-grants-2011_04