反応 #216021

ord-594dee8f56d74f84864d7c00003627d4

反応方程式

C=C(C)C(=O)O
methacrylic acid
[Na+].[OH-]
NaOH
C=C(C)C(=O)OC(=O)C(=C)C
Methacrylic Anhydride

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The 81A product (11.51 gm) was allowed to react under the conditions of Example 1 with 5.28 gm XSA, 9.99 gm methacrylic acid, 2.78 gm AMPS, and 44.50 gm water. After reaction, 6.94 grams of water was added along with NaOH to adjust pH to 4.4 (referred to below as 81B). The solution contained 29% solids.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05464911uspto-grants-1995_11