反応 #215693
ord-76ffd24e304642158af2cc014d8e9207
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
The synthesis of 6-bromo-2-tetralone is accomplished by dissolving 4-bromophenylacetic acid in methylene chloride and dimethyl formamide, under nitrogen. Oxalyl chloride is added and the mixture is stirred under a positive nitrogen atmosphere to produce the 4-bromo-phenylacetyl chloride, at a yield which typically is better than 99%.