反応 #215362

反応方程式

7-chloro-5-(2-fluorophenyl)-N-hydroxy-α-nitro-3H-1,4-benzodiazepine-2-methanimine

N-methylpiperazine

→

[7-Chloro-5-(2-fluorophenyl)-3H-1,4-benzodiazepin-2-yl](4-methyl-1-piperazinyl)methanone oxime

溶媒

tetrahydrofuran

反応条件

後処理

1. 1
   その他This compound was obtained
2. 2
   その他The analytical sample was recrystallized from ethanol, mp 198°-200° C.

実験手順

This compound was obtained by reacting 7-chloro-5-(2-fluorophenyl)-N-hydroxy-α-nitro-3H-1,4-benzodiazepine-2-methanimine with N-methylpiperazine in tetrahydrofuran. The analytical sample was recrystallized from ethanol, mp 198°-200° C.

出典