反応 #215335

ord-4077398a68c449bd94eb8bde13a2dfec

反応方程式

O=C(O)CCCCC(=O)O
adipic acid
CC(C)(CO)CO
neopentylglycol
O=C1CCC(=O)O1
succinic anhydride
CCCC(O)O
butanediol
C=Cc1ccc(C=C)cc1.C=Cc1ccccc1.c1ccc(COCC2CO2)cc1
Epoxide resin

反応条件

温度
120°CELSIUS
詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    workup.ADDITIONthe mixture is poured into Anticorodal moulds which
  2. 2
    温度have been pre-warmed to 140° C
  3. 3
    その他After removing the air
  4. 4
    その他Crystalline, soft and tough mouldings are obtained, on which the following characteristics

実験手順

77 g (0.05 equivalent) of an acid polyester prepared, by the melt process, from 21 mols of succinic anhydride and 20 mols of butanediol and 35 g (0.05 equivalent) of an acid polyester prepared, by the melt process, from 8 mols of adipic acid and 7 mols of neopentylglycol are warmed to 120° C. and mixed well with 11.0 g (0.1 equivalent) of triglycidyl isocyanurate and the mixture is poured into Anticorodal moulds which have internal dimensions of 150×150×1 mm, have been treated with a silicone mould-release agent and have been pre-warmed to 140° C. After removing the air, the mixture is cured in vacuo for 16 hours at 140° C. Crystalline, soft and tough mouldings are obtained, on which the following characteristics are determined:

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US04259198uspto-grants-1981_03