反応 #2146677

反応方程式

TEMPO

sodium bromide

Hydrogen peroxide

→

TEMPO H2O2

溶媒

water

反応条件

後処理

1. 1
   workup.ADDITIONA sample of cotton textile (ca. 1 g) is added to a solution
2. 2
   洗浄The material is washed with water
3. 3
   その他dried

実験手順

A sample of cotton textile (ca. 1 g) is added to a solution composed of 90 mL water with 10 mg (0.065 mmol) TEMPO and 0.22 g (2 mmol) sodium bromide. Hydrogen peroxide 3% is added (0.9 mL, 1 mmol) and the reaction stirred at RT for 10 minutes to 2 hours. The material is washed with water, dried, and used without further modification in the following ZnO deposition step.

出典