反応 #2139926

ord-30ba1818977d4670a24a24a0170e33ea

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    抽出The reaction mixture was extracted with ethyl acetate
  2. 2
    抽出the ethyl acetate extract
  3. 3
    洗浄was washed with water
  4. 4
    workup.DISTILLATIONfollowed by distillation in vacuo

実験手順

Ethyl vinyl ether was mixed in benzyl alcohol, to which was then added mercury acetate, and the mixture was stirred at room temperature for 12 hours. The reaction mixture was extracted with ethyl acetate and the ethyl acetate extract was washed with water, followed by distillation in vacuo to obtain benzyl vinyl ether.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US07326513B2uspto-grants-2008_02