反応 #2107

反応方程式

5-bromopentyl acetate

triethyl phosphite

→

5-(Diethylphosphono)pentyl acetate

反応条件

後処理

1. 1
   workup.DISTILLATIONThe mixture was then fractionally distilled under reduced pressure

実験手順

100.34 g (0.48 mol) of 5-bromopentyl acetate were heated at 150° C. for 8 hours with 79.8 g (0.048 mol) of triethyl phosphite while stirring and passing in nitrogen. The mixture was then fractionally distilled under reduced pressure.

出典