反応 #2063069

反応方程式

sodium hydroxide

behenic acid

arachidic acid

stearic acid

nitric acid

→

sodium behenate

溶媒

water

反応条件

後処理

1. 1
   workup.STIRRINGwith stirring for a period of 30 min.

実験手順

In 945 ml of water were dissolved 32.4 g of behenic acid, 9.9 g of arachidic acid and 5.6 g of stearic acid at 90° C. Thereafter, an aqueous 1.5M sodium hydroxide solution was added with stirring at a high speed. Subsequently, 0.93 ml of concentrated nitric acid was added thereto and cooled 55° C. with stirring for a period of 30 min. to obtain a sodium behenate solution.

出典