反応 #2063057

反応方程式

chlorobenzene

sodium carbonate

styrene

propylene carbonate

→

stilbene

溶媒

diethyl ether

反応条件

後処理

1. 1
   workup.ADDITIONis added
2. 2
   ろ過the mixture is filtered

実験手順

Under argon, a solution containing 122 mg of chlorobenzene, 106 mg of sodium carbonate, 157 mg of styrene and 1 ml of propylene carbonate stabilized 0.001 M colloid solution is heated at 155° C. with stirring in a sealed vessel for 17 h. At the end of the reaction, 2 ml of diethyl ether is added, and the mixture is filtered. The yield of isolated trans-stilbene is 15%.

出典