反応 #2063055

反応方程式

chlorobenzene

sodium carbonate

styrene

propylene carbonate

→

stilbene

溶媒

diethyl ether

反応条件

後処理

1. 1
   workup.ADDITIONis added
2. 2
   ろ過the mixture is filtered

実験手順

Under argon, a solution containing 122 mg of chlorobenzene, 229 mg of sodium carbonate, 141 mg of styrene and 1 ml of propylene carbonate stabilized colloid solution with a palladium content of 4.023 mg is heated at 155° C. with stirring in a sealed vessel for 65 h. At the end of the reaction, 2 ml of diethyl ether is added, and the mixture is filtered. The yield of desired product as determined by GC is 34%.

出典