反応 #2063053

反応方程式

2,3,3-trimethylindolenine

1,3-diiodopropane

→

1-[3-iodopropyl]-2,3,3-trimethyl-3H-indolium iodide

反応条件

後処理

1. 1
   その他The resulting solid is recrystallized from ethanol

実験手順

To a 50 mL round bottom flask is added 2,3,3-trimethylindolenine (14.4 mmol) and 1,3-diiodopropane (72.7 mmol) and the mixture is stirred at 60° C. under an atmosphere of nitrogen for 16 hours. The resulting solid is recrystallized from ethanol to give 1-[3-iodopropyl]-2,3,3-trimethyl-3H-indolium iodide (40) as crystals.

出典