反応 #2044336

ord-75e8b74a47d84092957d0a1eb590db9f

反応方程式

NCCC1CN(C(c2ccccc2)c2ccccc2)C1
3-aminoethyl-1-benzhydryl azetidine
CC(C)(C)OC(=O)NCC1CN(C(c2ccccc2)c2ccccc2)C1
3-(N-tert-butyloxycarbonylaminomethyl)-1-benzhydryl azetidine
→
CC(C)(C)OC(=O)NCCC1CN(C(c2ccccc2)c2ccccc2)C1
title compound
CC(C)(C)OC(=O)NCCC1CN(C(c2ccccc2)c2ccccc2)C1
3-(N-tert-butyloxycarbonylaminoethyl)-1-benzhydryl azetidine

反応物

NCCC1CN(C(c2ccccc2)c2ccccc2)C1
3-aminoethyl-1-benzhydryl azetidine
CC(C)(C)OC(=O)NCC1CN(C(c2ccccc2)c2ccccc2)C1
3-(N-tert-butyloxycarbonylaminomethyl)-1-benzhydryl azetidine

試薬

なし

反応条件

詳細条件
See reaction.notes.procedure_details.

実験手順

The title compound was prepared from 3-aminoethyl-1-benzhydryl azetidine according the procedure for 3-(N-tert-butyloxycarbonylaminomethyl)-1-benzhydryl azetidine, in a yield of 6.5 g (95%).

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05783563uspto-grants-1998_07