反応 #2021473

反応方程式

perfluorooctanesulfonic acid

silver carbonate

→

silver perfluorooctanesulfonate

溶媒

water

反応条件

後処理

1. 1
   workup.ADDITIONwas added
2. 2
   workup.STIRRINGAfter stirring at room temperature for 3 days
3. 3
   ろ過the mixture was filtered
4. 4
   ろ過the obtained filter-cake
5. 5
   洗浄was washed with 10 parts of ion-exchange water
6. 6
   乾燥20 parts of diethylether and dried

実験手順

Into a four-necked flask were charged 75 parts of perfluorooctanesulfonic acid and 100 parts of water, and 21.4 parts of silver carbonate was added thereto with stirring. After stirring at room temperature for 3 days, the mixture was filtered and the obtained filter-cake was washed with 10 parts of ion-exchange water, then 20 parts of diethylether and dried to give 60.3 parts of silver perfluorooctanesulfonate.

出典