反応 #2006428
ord-716a36f0ef684f5a928e9f76541cd645
反応方程式
sodium water glass
water
→
sodium silicate
試薬
なし
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
300 ml of sodium water glass was mixed with 2700 ml of de-ionized water to form an aqueous solution of sodium silicate, which was passed through a cationic exchange resin column, thereby forming silicic acid. 5 wt % aqueous KOH was added gradually at a temperature below 80° C. (preferably, 70-80° C.) until the pH value of the aqueous solution was greater than 10 so that the silicic acid was alkalized and under went polycondensation. The reaction product was cooled to 40° C., and was added with 300 ml of 10 wt % sodium aluminate aqueous solution. After 40 minutes, the reaction product was passed through a cationic exchange resin column to obtain a clear silica sol A.