反応 #1973963

反応方程式

3,4-dinitroaniline

methanesulfonyl chloride

pyridine

→

title compound

N-(3,4-dinitrophenyl)methanesulfonamide

溶媒

CH2Cl2

反応条件

後処理

1. 1
   濃縮Mixture was concentrated under vacuum

実験手順

A mixture of 3,4-dinitroaniline (5.27 g, 28.8 mmol), methanesulfonyl chloride (3.36 mL, 43.1 mmol) and pyridine (5.82 mL, 71.9 mmol) in CH2Cl2 (100 mL) was stirred for 24 h. Mixture was concentrated under vacuum to provide a crude semi-solid title compound that was used without further purification.

出典