反応 #1973929

ord-b5666bc56a9346019b9bca0b04b33190

反応方程式

CC(O)C(=O)[O-].CC(O)C(=O)[O-].[Ca+2]
calcium lactate
O.O=C(O)CC(O)(CC(=O)O)C(=O)O
citric acid monohydrate
CC(O)C(=O)O
lactic acid
O=C(O)CC(O)(CC(=O)O)C(=O)O
citric acid

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    workup.ADDITIONby adding
  2. 2
    その他was kept at 80° C. in order
  3. 3
    workup.DISSOLUTIONdissolved
  4. 4
    workup.ADDITIONby adding

実験手順

In a vessel, the following liquid (A) was prepared by adding and mixing 32 kg of water, 8 kg of Ca(OH)2 and 9.8 kg of lactic acid 88%. This liquid was kept at 80° C. in order to keep the calcium lactate dissolved and was continuously stirred to keep the excess Ca(OH)2 suspended. In an other vessel a citric acid solution was prepared by adding and mixing 50 kg of citric acid monohydrate and 32 kg of water.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US08501255B2uspto-grants-2013_08