反応 #1960480

反応方程式

stearic acid

sodium hydroxide

silver nitrate

→

silver stearate

溶媒

water

反応条件

後処理

1. 1
   workup.DISSOLUTIONwere completely dissolved
2. 2
   workup.STIRRINGthe result was stirred for 3 hours
3. 3
   その他White powder on the surface of the result was collected
4. 4
   洗浄washed three times each with distilled water

実験手順

7.5 g of stearic acid and 1.2 g of sodium hydroxide were added to 300 ml of water and sufficiently stirred until they were completely dissolved. 5.2 g of silver nitrate was added thereto, and the result was stirred for 3 hours. White powder on the surface of the result was collected and washed three times each with distilled water and with methanol to obtain silver stearate. An anode active material was prepared as in Example 1, except that silver stearate was used instead of nickel stearate, the molar ratio of silver to silicon was 0.2:1, the weight ratio of silicon to graphite was 0.5:1, and the carbon layer was 5.2 wt % of the anode active material.

出典