反応 #1947791

反応方程式

2′-aminomethylbiphenyl-2-carboxylic acid (3-methylbutyl)amide

methyl chloroformate

→

2′-(Methoxycarbonylaminomethyl)biphenyl-2-carboxylic Acid (3-Methylbutyl)amide

反応条件

後処理

1. 1
   抽出followed by extraction with EA and purification by flash chromatography 29 mg of 2′-(methoxycarbonylaminomethyl)-biphenyl-2-carboxylic acid (3-methylbutyl)amide
2. 2
   その他were obtained as a resin

実験手順

From 0.34 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid (3-methylbutyl)amide (precursor 5c) and methyl chloroformate, according to the general working procedure followed by extraction with EA and purification by flash chromatography 29 mg of 2′-(methoxycarbonylaminomethyl)-biphenyl-2-carboxylic acid (3-methylbutyl)amide were obtained as a resin.

出典