反応 #1947152

反応方程式

ethyl 3-[4-(2-azidoethoxy)phenyl]-2-(4-isopropylphenoxy)propionate

→

title compound

収率 91.4%

Ethyl 3-[4-(2-aminoethoxy)phenyl]-2-(4-isopropylphenoxy)propionate

収率 91.4%

反応条件

後処理

1. 1
   workup.ADDITIONthe reaction mixture was treated

実験手順

In a similar manner to that described in Reference example 1(d), a reaction was carried out using ethyl 3-[4-(2-azidoethoxy)phenyl]-2-(4-isopropylphenoxy)propionate (15.8 g), which is the product of Reference example 5(h), and palladium on carbon (5%, 1.60 g) and the reaction mixture was treated to afford the title compound (13.5 g) as a syrup.

出典