反応 #1929055
ord-4e127cdbee584fd48a1f74d53939a02e
反応方程式
16-azidohexadecanoic acid methyl ester
→
amine
16-aminohexadecanoic acid methyl ester
溶媒
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
16-azidohexadecanoic acid methyl ester is catalytically hydrogenated with palladium/activated charcoal in methanol at 3 bar for three hours to give the corresponding amine (Zinic et al., Positionally Isomeric Organic Gelators: Structure-Gelation Study, Racemic versus Enantiomeric Gelators, and Solvation Effects, Chem. Eur. J. 2010; 16:3066-82).