反応 #1925219
ord-3d314823161e4c64aa9131876a1f82ac
反応方程式
Pentafluorobenzenesulfonyl chloride
tetramethylammonium hydroxide
→
tetramethylammonium pentafluorobenzenesulfonate
溶媒
反応条件
詳細条件
See reaction.notes.procedure_details.
実験手順
Pentafluorobenzenesulfonyl chloride (25 g) was dissolved in 100 ml of methanol under ice cooling, and 100 g of a 25% aqueous solution of tetramethylammonium hydroxide was slowly added thereto, followed by stirring at room temperature for 3 hours. Thus, a solution of tetramethylammonium pentafluorobenzenesulfonate was obtained. This solution was used for salt interchange with a sulfonium salt and an iodonium salt.