反応 #1922851

反応方程式

pentafluorobenzenesulfonyl chloride

tetramethylammonium hydroxide

→

pentafluorobenzenesulfonic acid tetramethylammonium salt

溶媒

methanol

反応条件

実験手順

25 g of pentafluorobenzenesulfonyl chloride was dissolved in 100 mL of methanol under ice cooling, and 100 q of a 25% tetramethylammonium hydroxide aqueous solution was gradually added to the solution. The mixture was stirred at room temperature for 3 hours to obtain a solution of pentafluorobenzenesulfonic acid tetramethylammonium salt. This solution was used for salt exchange with sulfonium salt and iodonium salt.

出典