反応 #1916761
ord-77186be32eb642ce83ed149c509343aa
反応方程式
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他Unreacted SOCl2 is evaporated
実験手順
180.93 g (0.400 mol) di(pentafluorophenyl)diethoxysilane, 29 mL (0.400 mol, 47.6 g) thionylchloride and 4.92 g (0.0426 mol) pyridinium hydrochloride are refluxed and stirred for 16 h. Unreacted SOCl2 is evaporated and di(pentafluorophenyl)chloroethoxysilane isolated by vacuum distillation.