反応 #1914811

反応方程式

3-methyl-1,4-benzoquinone-4-oxime

acetic anhydride

→

3-methyl-1,4-benzoquinone-4-(O-acetyloxime)

溶媒

反応条件

後処理

1. 1
   その他At the end of the reaction
2. 2
   ろ過The precipitated product was filtered off
3. 3
   洗浄washed with water
4. 4
   その他dried

実験手順

One drop of pyridine was added to a mixture of 0.5 g (3.6 mmol) of 3-methyl-1,4-benzoquinone-4-oxime and 1 mL of acetic anhydride and the resulting mixture was heated to 70° C. At the end of the reaction, the reaction mixture was poured on 10 mL of water/ice. The precipitated product was filtered off, washed with water and then dried.

出典