反応 #1885010
ord-84a817739218448f800ce098b60147f5
反応方程式
styrene
butyl acrylate
acrylic acid
dodecanethiol
sodium dodecylbenzenesulfonate
→
Styrene Butyl Acrylate Acrylic Acid
溶媒
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他In a reactor equipped with a reflux condenser, a stirrer
- 2workup.ADDITIONa nitrogen-introducing pipe
実験手順
In a reactor equipped with a reflux condenser, a stirrer, a nitrogen-introducing pipe, and a monomer dripping funnel, 3.3 parts of sodium dodecylbenzenesulfonate is dissolved in 3,824 parts of ion exchange water. Subsequently, 30.6 parts of styrene, 9.4 parts of butyl acrylate, 1.2 parts of acrylic acid dimer, and 0.3 parts of dodecanethiol are added thereto, and thoroughly stirred at room temperature for emulsification stabilization (emulsified liquid 1).