反応 #1884970

反応方程式

1-methoxymethylcyclopropylsulfonylamine tert-butyl-carbamate

n-propyl isocyanate

→

1-propylcarbamoylcyclopropanesulfonamide tert-butylcarbamate

収率 100.0%

反応条件

後処理

1. 1
   その他This compound was obtained in a crude 100% yield
2. 2
   その他The compound was taken directly into the next reaction without purification

実験手順

This compound was obtained in a crude 100% yield according to the procedure described for the synthesis of 1-methoxymethylcyclopropylsulfonylamine tert-butyl-carbamate except that 1.10 equivalents of n-propyl isocyanate was used as the electrophile. The compound was taken directly into the next reaction without purification: 1H NMR (CDCl3) δ 0.10 (m, 2H), 0.51 (m, 2H), 0.67 (m, 1H), 1.10 (m, 2H), 1.49 (s, 9H), 1.62 (m, 2H), 1.87 (d, J=7.0 Hz, 2H).

出典