反応 #1880949
ord-e3da1ad9914a4f978033cb83e4daf5c9
反応方程式
Cyclohexylethyl alcohol
ethyl vinyl ether
→
cyclohexylethyl vinyl ether
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他The resultant reaction mixture
- 2抽出was extracted with ethyl acetate and water
- 3洗浄the extract was washed with water
- 4workup.DISTILLATIONdistilled under reduced pressure
実験手順
Cyclohexylethyl alcohol was mixed with ethyl vinyl ether. Mercury acetate was added thereto and this mixture was stirred at room temperature for 12 hours. The resultant reaction mixture was extracted with ethyl acetate and water, and the extract was washed with water and then distilled under reduced pressure to obtain cyclohexylethyl vinyl ether (X-1) as the target compound.