反応 #1876821
ord-a9e2bc7ece64422aa680ac0d6978bd7c
反応方程式
1,3-dichloroformyl-5-hydroxyadamantane
trimethylamine
trimethylsilyl chloride
→
1,3-dichloroformyl-5-trimethylsiloxyadamantane
反応条件
詳細条件
See reaction.notes.procedure_details.
後処理
- 1その他Reaction
- 2その他was carried out at room temperature
実験手順
The 1,3-dichloroformyl-5-hydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an eguimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature to obtain 1,3-dichloroformyl-5-trimethylsiloxyadamantane.