反応 #1876820

反応方程式

1,3,5-trihydroxyadamantane

trimethylamine

trimethylsilyl chloride

→

1,3-dihydroxy-5-trimethylsiloxyadamantane

溶媒

methylene chloride

反応条件

後処理

1. 1
   その他Reaction
2. 2
   その他was carried out at room temperature
3. 3
   その他The reaction product was partitioned by high performance liquid chromatography

実験手順

This 1,3,5-trihydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an equimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature. The reaction product was partitioned by high performance liquid chromatography to obtain 1,3-dihydroxy-5-trimethylsiloxyadamantane.

出典