反応 #1869202

反応方程式

1,1-dimethylethyl {1-[2-(4-quinolinyl)ethyl]-4-piperidinyl}carbamate

chloroform

→

product

収率 100.0%

1-[2-(4-quinolinyl)ethyl]-4-piperidinamine trihydrochloride

収率 100.0%

溶媒

HCl

dioxane

反応条件

後処理

1. 1
   その他the reaction mixture was evaporated to dryness

実験手順

1,1-dimethylethyl {1-[2-(4-quinolinyl)ethyl]-4-piperidinyl}carbamate (9a) (278 mg) was dissolved in chloroform and diluted with 4N HCl in dioxane solution. After stirring two hours, the reaction mixture was evaporated to dryness to afford the product as a solid (180 mg, 100%).

出典