反応 #1855696

ord-d5ecc4ec14794b97a139a22354e972dd

反応条件

詳細条件
See reaction.notes.procedure_details.

後処理

  1. 1
    その他the mixture was reacted at 30° C. for 1 hour

実験手順

OA (manufactured by Sigma Co., 30 mg) was dissolved in 0.1M phosphate buffer (pH 7.0 , 1 ml), thereto was added an NHS-LC-biotin solution (manufactured by Pierce Chemical Co., 12.6 mg/ml 0.1M phosphate buffer, pH 7.0; 100 μl) and the mixture was reacted at 30° C. for 1 hour. Thereafter, the procedure in Example 5 (a) was repeated to give a biotin-OA fraction.

出典

DOI: 10.6084/m9.figshare.5104873.v1特許: US05378608uspto-grants-1995_01